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title
organicmethodology
description
Just another WordPress.com site
image
site name
organicmethodology
author
updated
2026-02-20 12:17:52
raw text
organicmethodology | Just another WordPress.com site organicmethodology Just another WordPress.com site Main menu Skip to content MMOR OPRD Journals Chemfeeds ChemLinks Org Chem Info ACS Links Orgsyn Patents Reactions Scientificupdate Post navigation Dec 16 2011 Development of a Scalable Synthesis of a GPR40 Receptor Agonist Shawn D. Walker,* Christopher J. Borths, Evan DiVirgilio, Liang Huang, Pingli Liu, Henry Morrison, Kiyoshi Sugi, Masahide Tanaka, Jacqueline C. S. Woo, and Margaret M. Faul Org. Process Res. Dev . , 2011, 15 , 570–580 DOI: 10.1021/op1003055 Summary: AMG 837 is a novel GPR40 receptor agonist developed at Amgen. The end game of the synthesis involved an alkylative coupling between ( S )-3-(4-hydroxyphenyl)hex-4-ynoic acid ( 1 ) and 3-(bromomethyl)-4′-(trifluoromethyl)biphenyl ( 2 ). The chiral non-racemic acid (1) (bottom left) was prepared in 35% overall yield via a classical resolution utilizing the amino a...
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