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title
Org Prep Daily
description
synthetic procedures I tried and liked
image
site name
Org Prep Daily
author
updated
2026-02-27 12:32:30
raw text
Org Prep Daily | synthetic procedures I tried and liked Org Prep Daily April 6, 2019 Sodium trans-[tetrachloro Bis-(1H-Indazole)-Ruthenate(III)] dihydrate Filed under: procedures — milkshake @ 9:30 am Sodium sulfate 213.0 g (anhydrous, 3.0 mol of Na) was gradually added into a stirred slurry of Al2(SO4)3 .18H2O 1000g (3.0 mol of Al) in D.I. water 2L and the mixture was stirred to complete dissolution (about 30 min). The total volume was adjusted by addition of D.I. water to 2.7L and the solution was filtered through a fine porosity filter. The obtained 1.1M solution of NaAl(SO4)2 was combined with 226.9g of the Cs salt (350 mmol) in a large 4L beaker. Solid CsCl 6g was added to the stirred mixture, to seed the formation of cesium alum CsAl(SO4)2.12H2O crystals. The mixture was stirred in open Erlenmeyer flask at ambient temperature for 30 hours. During this time, the red-brown slurry of the cesium salt turned into coffee-brown black slurry of the sodium salt intermix...
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